Narrated `Abdullah: The first Sura in which a prostration was mentioned, was Sura An-Najm (The Star). Allah's Messenger (ﷺ) prostrated (while reciting it), and everybody behind him prostrated except a man whom I saw taking a hand-full of dust in his hand and prostrated on it. Later I saw that man killed as an infidel, and he was Umaiya bin Khalaf.
Source: sunnah.com
Other translations
Arabic
حَدَّثَنَا نَصْرُ بْنُ عَلِيٍّ، أَخْبَرَنِي أَبُو أَحْمَدَ، حَدَّثَنَا إِسْرَائِيلُ، عَنْ أَبِي إِسْحَاقَ، عَنِ الأَسْوَدِ بْنِ يَزِيدَ، عَنْ عَبْدِ اللَّهِ ـ رضى الله عنه ـ قَالَ أَوَّلُ سُورَةٍ أُنْزِلَتْ فِيهَا سَجْدَةٌ {وَالنَّجْمِ}. قَالَ فَسَجَدَ رَسُولُ اللَّهِ صلى الله عليه وسلم وَسَجَدَ مَنْ خَلْفَهُ، إِلاَّ رَجُلاً رَأَيْتُهُ أَخَذَ كَفًّا مِنْ تُرَابٍ فَسَجَدَ عَلَيْهِ، فَرَأَيْتُهُ بَعْدَ ذَلِكَ قُتِلَ كَافِرًا، وَهْوَ أُمَيَّةُ بْنُ خَلَفٍ.
sunnah.com